Oxide Crucibles for Precious Metals--cs ceramic co.,ltd
Many of the precious metal group of non-ferrous metals can be melted adequately in clay-graphite or silicon carbide crucibles, but for melting temperatures above 1400oC..and for higher quality casts...then oxide crucibles should be used.
Oxide crucibles for precious metals are normally made by isostatic pressing, but for special shapes and non-standard sizes the equivalent material can be formed by vibro-casting.
Zirconia (zirconium oxide) is the material of choice, and several grades are available. A cheaper alternative is zircon (zirconium silicate) which is often used for refining platinum-group alloys from glassy material.
The usual arrangement is to prepare an assembly with the crucible packed into a refractory sleeve with a granular backing mix. The sleeve can be of a lower quality refractory compared to the crucible as it only reaches a fraction of the temperature seen by the crucible; its main qualities should be high strength and good thermal flexibility to accommodate thermal expansion of its’ contents during multiple thermal cycles.
A slow pre-heat schedule should be followed, and if the crucible is allowed to cool towards room temperature between casts the pre-heat schedule should be followed again.
- See more at: http://www.csceramic.com/csceramic/product/list.asp?c=fire%20assay%20crucible&subc=all#sthash.wIrFahOF.dpuf |